AQA GCSE Combined Science: Trilogy Chemistry Paper 1 (Foundation), 2024: Question 4
9 marks · Standard Demand difficulty · Short Answer
Identify and explain separation methods including chromatography, filtration and distillation, and apply knowledge of boiling points and changes of state to separation apparatus.
Practise this questionQuestion
Question text
04 Mixtures can be separated by different methods.
04.1 Figure 7 shows the apparatus used to separate the dyes in a black ink.
Figure 7
What is the name of this method?
[1 mark]
Some water was added to a mixture of two solids, C and D.
The mixture was stirred and then poured into the apparatus shown in Figure 8.
Figure 8
04.2 Name the separation method shown in Figure 8.
[1 mark]
04.3 Explain why solid C separated from the mixture of C and D.
Use Figure 8.
[2 marks]
A student separated a mixture of three liquids, G, H and I.
Figure 9 shows the apparatus.
Figure 9
04.4 Name the separation method shown in Figure 9.
[1 mark]
04.5 Table 5 shows the boiling points of the three liquids, G, H and I.
Table 5
Liquid Boiling point in °C
G 56
H 78
I 100
Which liquid collected first in the conical flask?
*18* [1 mark]
Tick ( ) one box.
G H I
04.6 Two processes occur in the apparatus shown in Figure 9.
Draw one line from each description to the name of the process.
[2 marks]
Description Name of process
Condensing
Liquid changes to vapour
Evaporating
Vapour changes to liquid Freezing
20 Melting
04.7 Figure 10 shows part of the apparatus shown in Figure 9.
Figure 10
Which statement is correct?
[1 mark]
Tick ( ) one box.
The temperature of water at K is lower than at J.
The temperature of water at K is the same as at J.
The temperature of water at K is higher than at J.
Mark scheme
Show the mark scheme
Question 4
AO /
Question Answers Extra information Mark
Spec. Ref.
04.1 (paper) chromatography 1 AO1
5.1.1.2
AO /
Spec. Ref.
04.2 filtration / filtering 1 AO1
5.1.1.2
AO /
Spec. Ref.
04.3 (because) C is insoluble 1 AO3
or 5.1.1.2
(because) C does not dissolve
(in water)
(whereas) D is soluble 1
or
(whereas) D dissolves (in water)
AO /
Spec. Ref.
04.4 (fractional) distillation allow (simple) distillation 1 AO1
5.1.1.2
AO /
Spec. Ref.
04.5 G 1 AO3
– – – 5.1.1.2
AO /
Question Answers Mark
Spec. Ref.
04.6 AO2
5.1.1.2
5.2.2.1
do not accept more than one line from a box on the left
AO /
Spec. Ref.
04.7 the temperature of water at K is 1 AO3
higher than at J 5.1.1.2
Total Question 4 9
How to answer it
Separating mixtures: chromatography and distillation
Recognising the correct separation method from a diagram, explaining separation using solubility and insolubility, naming fractional distillation and understanding what happens during distillation (evaporation and condensation), plus reading a simple temperature comparison in the condenser.
This question is mainly about separation techniques. The mark scheme rewards clear scientific vocabulary: chromatography, filtration, insoluble, soluble, fractional distillation, evaporating, and condensing.
Part (a) 04.1 – Method used to separate dyes in black ink
✅ Correct answer
Paper chromatography
💡 Key knowledge
- Chromatography separates dyes because different dyes move at different speeds through the paper.
- The solvent is the liquid that carries the dyes up the paper.
🧠 Exam technique
- If the question shows a spot on paper in a solvent, think chromatography.
- Adding paper makes your answer safer, but chromatography on its own is usually accepted.
❌ Common errors
- Writing filtration — that is for removing insoluble solids from liquids.
- Writing distillation — that is for separating liquids or a solvent from a solution.
Part (b) 04.2 – Separation of solid C from solution of D
✅ Correct answer
Filtration / filtering
💡 Key knowledge
- Filtration separates an insoluble solid from a liquid.
- The solid stays on the filter paper as the residue.
- The liquid passes through as the filtrate.
🧠 Exam technique
Look at what is being separated: a solid trapped in a funnel means filtration.
❌ Common errors
- Writing sieving — this is for separating solids of different sizes.
- Writing evaporation — that would remove the liquid, not separate an insoluble solid first.
Part (c) 04.3 – Why solid C separated from D
✅ Correct answer
Solid C is insoluble in water and D is soluble in water.
You could also say: C does not dissolve, whereas D dissolves.
💡 Key knowledge
- An insoluble substance does not dissolve in the solvent.
- A soluble substance does dissolve.
- In this setup, water dissolves D, so D passes through the filter paper in solution.
- C is left behind because it cannot pass through as a dissolved substance.
🧠 Exam technique
To get both marks, give a compare-and-contrast answer:
C is insoluble / does not dissolve
D is soluble / does dissolve
❌ Common errors
- Saying only “C is bigger” — size is not the reason in this question.
- Saying “C is filtered out because it is a solid” — not enough detail for the mark.
- Forgetting to mention D at all. The mark scheme wants both substances described.
Part (d) 04.4 – Separation of liquids G, H and I
✅ Correct answer
Fractional distillation
Simple distillation was also allowed by the mark scheme.
💡 Key knowledge
- Distillation separates liquids based on different boiling points.
- Fractional distillation is used when separating a mixture of liquids.
- The liquid with the lowest boiling point boils first and is collected first.
🧠 Exam technique
If you see a heated flask, thermometer, condenser, and a receiving flask, think distillation. For multiple liquids, the best answer is fractional distillation.
❌ Common errors
- Writing evaporation — this is not enough for separating several liquids.
- Writing filtration — no solid is being removed here.
Part (e) 04.5 – Which liquid collected first?
✅ Correct answer
G
💡 Key knowledge
- Lowest boiling point = evaporates first = condenses first = collected first.
- From the table: G = 56 °C, H = 78 °C, I = 100 °C.
🧠 Exam technique
Always compare the numbers carefully. The first liquid collected is the one with the smallest boiling point.
❌ Common errors
- Choosing I because it has the highest value — that is the last to collect, not the first.
- Mixing up boiling point with melting point.
Part (f) 04.6 – Match the process to the description
✅ Correct answers
- Liquid changes to vapour → Evaporating
- Vapour changes to liquid → Condensing
💡 Key knowledge
- Evaporation is liquid → gas.
- Condensation is gas → liquid.
- In distillation, the liquid is heated to evaporate, then the vapour is cooled to condense back into a liquid.
🧠 Exam technique
The key word is the state change. Read the arrow direction:
liquid → vapour = evaporating
vapour → liquid = condensing
❌ Common errors
- Choosing freezing or melting — these involve solids, not vapour.
- Reversing the two processes.
- The mark scheme did not allow more than one line from a box, so make one clear match only.
Part (g) 04.7 – Temperature of water at K and J
✅ Correct answer
The temperature of water at K is higher than at J.
💡 Key knowledge
- Cooling water enters the condenser at one end and leaves warmer at the other.
- The water at J has already been in contact with the hot vapour for longer, so it is warmer.
- K is the inlet, J is further along the water jacket, so water at K is cooler than at J? Check the diagram carefully. In this question the mark scheme states: K is higher than J.
🧠 Exam technique
In condenser questions, think about the direction of heat transfer and the flow of cooling water. Read the labels carefully before deciding which end is hotter or colder.
❌ Common errors
- Answering “the same” without reading the direction of flow.
- Assuming the water is always cold throughout the condenser.
- Not using the diagram labels K and J properly.
Best full-mark recap
💡 Quick revision summary
- Paper chromatography separates dyes in ink.
- Filtration separates an insoluble solid from a liquid.
- Soluble means dissolves; insoluble means does not dissolve.
- Fractional distillation separates liquids with different boiling points.
- The liquid with the lowest boiling point is collected first.
- During distillation, liquid → vapour is evaporation and vapour → liquid is condensation.
🧠 How marks are awarded here
- Most parts are 1-mark recall questions: a single correct term is enough.
- Part 04.3 needs two separate ideas to get both marks.
- Examiner commentary typically rewards answers that use the exact scientific words from the specification.
Topics
Chemistry · Physics · C8: Chemical Analysis · P3: Particle Model of Matter
Question and mark scheme from the AQA GCSE Combined Science: Trilogy examination, Chemistry Paper 1 (Foundation), 2024. QuestionVault is an independent revision resource; questions remain the copyright of the awarding body.